fabrication and characterization of natural fiber reinforced composite
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newline ABSTRACT
newlineIn recent years utilization of nature-based materials has become a matter of immense concern due
newlineto increasing environmental awareness in terms of sustainability, safety and maintaining ecological
newlinebalance.
newlineReinforcement of natural fibers has established a strong alternative to replace synthetic fibers for
newlinethe production of polymer composite materials. Bio- materials are being used now a days in every
newlinepossible field of engineering. These bio- based materials include plant based natural fibers like
newlinesisal , jute , flax, hemp, ramie , coir , oil-palm etc. , animal fibers like silk, wool, angora etc. These
newlinefibers are reinforced with polymer to fabricate bio- composites.
newlineBio- composites have ignited the minds of various material scientists to be used in various
newlineindustries like automobile, aerospace, marine, textile and sports. Application areas of natural fiber
newlinereinforced composites are spreading in every field of engineering having structural and nonstructural
newlineapplications.
newlineThe current research work aims at highlighting the issues and challenges associated with
newlineprocessing of plant based thermoset composite. In this work, natural fiber i.e., Sisal and Flax were
newlinereinforced with epoxy matrix to fabricate natural fiber reinforced composite (NFRC). The hand
newlinelay-up technique was used for the fabrication using compression molding machine. Developed
newlinecomposites were characterized for their physical properties, mechanical properties and
newlineTribological properties.
newlineSisal fiber was reinforced with epoxy matrix in four conditions (i) without any chemical treatment
newline(Type A composites) (ii) sisal was treated with 4% NaOH solution (type B) (iii) Sisal was treated
newlinewith 10% NaOH solution (Type C) (iv) Hybrid composite (Type D) was formed with Sisal and
newlinexii
newlineFlax. Hand-lay-up technique was used for the fabrication of the composites using cold mold of
newlinemild steel. Developed composite were characterized for their chemical properties, physical
newlineproperties, mechanical properties and Tribological properties.
newlinePhysical properties (density), chemical characterization (FTIR Spectroscopy and X-Ray
newlineDiffraction) and thermal analysis (TGA and DTA) of untreated composite, 4% treated composite,
newline10% treated composite and Flax and Sisal hybrid composites were performed. For the density
newlinecalculations Archimedes principle was used. FTIR spectroscopy shows the presence of
newlinehemicellulose, cellulose, lignin and pectin in the composites. DTA test is performed to understand
newlinethe type of polymerization process (endothermic or exothermic). TGA test is performed to
newlineunderstand the thermal stability of the composites.
newlineMechanical properties (Tensile, Compression, Flexural, Impact, Hardness) for untreated
newlinecomposites, treated composites and hybrid composites were evaluated. The effect of chemical
newlinetreatment and mixing of another natural fiber (Flax) were investigated. SEM micrographs of
newlinefractured surfaces after mechanical characterization were analyzed to reveal the surface condition
newlineand possible mechanism of failure. Tensile tests concluded that maximum tensile strength was
newlineachieved by hybrid (flax and Sisal) composite i.e., type D which was 29.98 MPa. Compression tests
newlineconcluded that maximum compressive strength was achieved by chemically treated Sisal fiber (4%
newlineNaOH) treated composites i.e., Type B. Maximum flexural strength was achieved by treated Sisal
newlinefiber (4% NaOH) reinforced composites i.e., Type B. All composites were undergone for hardness
newlineand impact testing and it was concluded that maximum flexural strength was achieved by treated
newlineSisal (4% NaOH) reinforced composites i.e., type B which was 82.646 MPa. Impact test was done
newlineon Automatic Impact tester and it was concluded that maximum Impact strength was achieved by
newlinexiii
newlinehybrid composites (Flax and Sisal). Hardness tests were done on Shore D hardness teste. Hardness
newlineresults for all types of composites varied from 74 to 82.
newlineTribological performance of the developed bio-composites were evaluated for conditions
newlinementioned above in terms of frictional characteristics and sliding wear and dry contact condition
newlineat different process parameters such as applied load (20N to 60N), sliding distance(0-700m) and
newlinetime period for which observations were made was 5 minutes, 10 minutes and 15 minutes.
newlineExperimental results of wear Analysis confirmed that type A composites attained the maximum
newlinewear rate. Specific wear rate (SWR) decreases from type B to type C composites which means
newlinethat as the concentration of chemical treatment increases, specific wear rate decreases and hybrid
newlinecomposite gets greater SWR than SFRC.